海山富钴结壳标准物质研制

王毅民; 高玉淑; 王晓红; 张学华; 赵宏櫵; 刘淑琴; ANDREEVSI

海山富钴结壳标准物质研制

1.
国家地质实验测试中心, 北京 100037
2.
广州海洋地质调查局, 广东广州 510760
3.
国家海洋局第二海洋研究所, 浙江杭州 310012
4.
中国地质科学院矿产资源研究所, 北京 100037
5.
俄罗斯大洋地质与矿产资源研究所, 圣彼得堡 191021

基金项目: "大洋矿产资源研究与开发"国家专项资助项目(DY95-05-03)

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出版历程
- 收稿日期: 2006-03-28
- 修回日期: 2006-08-21

A series of seamount cobalt-rich crust reference materials

1.
National Research Center of Geoanalysis, Beijing 100037, China
2.
Guangzhou Marine Geological Survey, Guangzhou 510760, China
3.
Second Institute of Oceanography, State Oceanic Administration, Hangzhou 310012, China
4.
Institute of Mineral Resources, Chinese Academy of Geological Sciences, Beijing 100037, China
5.
All-Russian Research Institute for Geology and Mineral Resources of the World Ocean(VNIIOkeangeologiya), St Petersburg 191021, Russia

摘要

摘要: 报道了我国与俄罗斯合作研制的三个海山富钴结壳标准物质GSMC-1,2,3.这三个标准物质的原样分别取自西太平洋麦哲伦海山和中太平洋海山.样品经风干、选配、球磨制备成均匀的粉体样品,其均匀性采用高精度的X-射线荧光光谱法检验.样品的化学组分采用国内外多实验室协同分析方式定值,有八个国内实验室和八个国外实验室参加了合作分析.测试组分均为57个,其中GSMC-1,2有43个组分定为保证值,10个组分作为参考值;GSMC-3有45个组分定为保证值,8个组分作为参考值.经2a多的试用,三个标准物质已于2005年被国家计量部门批准为国家一级标准物质,其编号分别为GBW07337,GBW07338和GBW07339.
- 标准物质 /
- 富钴结壳 /
- 化学成分 /
- 太平洋海山
Abstract: The collaborative preparation of three seamount cobalt-rich crust reference materials GSM C-1~3 by China and Russia is presented.The samples were sampled from the western and central Pacific seamount zones.After the raw samples were dried in ambient air and crushed,they were ground in a ball mill to form a well-mixed powder.The homogeneity of the samples wastested using X-ray fluo rescence spectrometry(XRF) with high-precision.Eight home laboratories and eight international laboratories participated in the collaborative analysis programme.Fifty-seven elements or constituents were analy sed,and among those,43 were certified in GSM C-1 and 2,and 45 const it uents were certified in GSMC-3.Ten constituents were regarded as information value in GSM C-1 and 2,and eight const ituents were regarded as information value in GSM C-3.These three reference materials have been approved as certified reference materials by the Administ ration of Quality Supervision and Inspection and Quarantine(AQSIQ,China) in 2005,the serial number is GBW07337 for GSM C-1,GBW07338 for GSM C-2 and GBW07339 for GSM C-3.
- reference materials /
- cobal-trich crust /
- chemical constituents /
- Pacific seamounts

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参考文献(28)

HALBACH P,MANHEIM F T.Potential of cobalt and other metals in ferromanganese crusts on seamounts of the Central Pacific basin[J].Marine Mining,1984,4(4):319-336.

MANHEIM F T.Marine cobalt resource[J].Science,1986,232:600-608.

MANHEIM F T,LANE-BOSTWICK C M,Chemical Composition of Ferro-manganese Crusts in the World Ocean,US Geol Surv Openfile Rep,89-020[R].Washengton DC:USGS,1989.475.

BERKOVITS L A,OBOLYANINOVA V G,BATURIN G N.Standard samples of iron-manganese nodules and surrounding sediments[J].Oceanology,1990,30:329-335.

G0VINDARAJU K.Compilation of working values and samples description for 383 geostandards[J] Geost Newsl,1994,18 (Special Issue):1-158.

许东禹.中太平洋海山区富钴锰结壳的研究[J].海洋地质与第四纪地质,1986,6(1):65-74.

王晓红,滕云业,潘家华,等.约翰斯顿岛附近海山富钴锰结壳的元素组成及地球化学特征[J].地球学报.2000,21(3):282-286.

WANG Yi-min,SONG Hao-wei,WANG Xiao-hong.Ocean manganese nodule and sediment reference materials[J].Marine Georesources & Geotechnology,1998,16(4):321-334.

王毅民,滕云业,罗代洪,等.大洋多金属结核及深海沉积物标准物质研制工作简述[J].岩矿测试,1997,16(3):161-169.

JJG 1006-94,一级标准物质[S].

HALBACH P,SEGL M,PUTEANUS D,et al.Co-fluxes and growth rates in ferromanganese deposits from central Pacific seamount areas[J].Nature,1983,304(5 928):716-719.

ISO GUIDE 30:1992 Terms and Definitions Used in Connection with Reference Materials(2nd ed.)[S].

ISO GUIDE 34:2000 Quality System Guidelines for the Production of Reference Materials[S].

钱耆生,沈国超.化工产品质量保证[M].北京:中国计量出版社,1994.195-430.

KANE J S,POTTS P J,WIEDENBECK M,et al.International association of geoanalysts' protocol for the certification of geological and environmental reference materials[J].Journal of Geostandards and Geoanalysis,2003,27 (3):227-244.

高玉淑,王晓红,王毅民."地质分析"国际会议及"国际地质分析者协会"简介[J].岩矿测试,2001,20(4):299-300.

FLANAGAN F J,GOTTFRIED D.USGS rock standards:Ⅲ.Manganese nodule reference samples USGS-Nod-A-1 and USGS-Nod-P-1[A].USGS Professional Paper 1155[C].Washington D C:Government Printing Office,1980.

BERKOVITS L A,OBOLYANINOVA V G,PARSHIN A K,et al.A system of sediment reference samples:OO[J].Geostandards Newsletter,1991,15:85-109.

TERASHIMA S,USNI A,IMAI N.Two new GSJ geochemical reference samples Synite JSy-1 and manganese nodule JMn-1[J].Geostandards Newsletter,1995,19:221-229.

WANG Yi-min,LUO Dai-hong,GAO Yu-shu,et al.A preliminary study on the preparation of four Pacific Ocean polymetallic nodule and sediment reference materials:GSPN-2,GSPN-3,GSMS-2 and GSMS-3[J].Geostandards Newsletter,1998,22(2):247-255.

CHEN Guo-fang,WANG Ji-wu.The preparation of marine geochemical certified reference materials-polymetallic nodule GSPN-1 and marine sediment GSMS-1 from the Pacific Ocean[J].Geostandards Newsletter,1998,22(1):119-125.

LI Ji-le,LIU Wen-zhang.The influence of chlorine on the determination of combined water:an investigation of a correction procedure[J].Geostandards Newsletter,1998,22(2):203-208.

王毅民,王晓红,张学华.富钴锰结壳分析技术评介[J].岩矿测试,1998,17(4):306-311.

HODGE V F,STALLARD M,KOIDE M,et al.Platinum and platinum anomaly in the marine environment[J].Earth and Planetary Sci Lett,1985,72:158-162.

王晓红,詹秀春,黄宇营,等.SR-XRMP研究海山富钴结壳微构造的元素分布特征[J].核技术,2005,28(11):810-814.

HEIN J R,KOSCHINSKY A,HALLIDAY A N.Global occurrence of tellurium-rich ferromanganese crusts and model for the enrichment of tellurium[J].Geochimica et Cosmochimica Acta,2003,67(6):1 117-1 127.

王毅民,王晓红,宋浩威,等.太平洋锰结核及沉积物的平均化学组成[J].自然科学进展,1999,9(10):918-924.

王晓红,高玉淑,王毅民.超细地质标准物质及其应用[J].自然科学进展,2006,16(3):309-315.

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